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doi: 10.1007/s00281-019-00745-4 54 JourdanTGodlewskiGCinarRBertolaASzandaGLiuJet al

& Palomaki, G

[] d = + 37.7 (c = 0.13, CHCl 3 ), Rf = 0.37 (hexane/acetone 6/4), 1 H NMR (400 MHz, CDCl 3 ) (ppm) 7.75 (d, J = 8.3 Hz, 1 H), 7.56 (d, J = 8.1 Hz, 1 H), 7.387.14 (m, 23 H), 7.02 (d, J = 8.0 Hz, 1 H), 6.92 (d, J = 7.6 Hz, 1 H), 5.35 (s, 1 H), 5.07 (s, 1 H), 5.00 (s, 1 H), 4.81 (d, J = 6.4 Hz, 1 H), 4.77 (d, J = 2.1 Hz, 1 H), 2.42 (s, 3 H, Ts C H 3 ), 1.48, 1.28 (2 x s, 2 3 H, 2 x i -propylidene C H 3 )